4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

Base Information

Chemical Name:4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester
CAS No.:1359296-25-5
Molecular Formula:C₁₉H₂₈O₆
Molecular Weight:352.428
Hs Code.:

Synonyms:4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

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Chemical Property of 4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

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Technology Process of 4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

There total 5 articles about 4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.8%

: 67-56-1
methanol

: 1359296-33-5
4,6-bis(3-methylbutoxy)isophthalic acid

: 1359296-25-5
4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

Guidance literature:: methanol; 4,6-bis(3-methylbutoxy)isophthalic acid; With sodium hydroxide; In water; at 20 ℃; for 4h; Reflux;

With hydrogenchloride; In water;
DOI:10.1039/c2cc16912f

Reference yield:

: 1359296-31-3
4,6-bis(3-methylbutoxy)isophthalic acid dimethyl ester

: 1359296-25-5
4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / methanol / 5 h / Reflux

2: sodium hydroxide / water / 4 h / 20 °C / Reflux

With water; sodium hydroxide; In methanol; water;
DOI:10.1039/c2cc16912f

Reference yield:

: 52959-28-1
dimethyl 4,6-dihydroxyisophthalate

: 1359296-25-5
4,6-bis(3-methylbutoxy)isophthalic acid monomethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 100 °C

2: water; sodium hydroxide / methanol / 5 h / Reflux

3: sodium hydroxide / water / 4 h / 20 °C / Reflux

With water; potassium carbonate; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c2cc16912f