deoxybenzoin o-methoxyphenylhydrazone

Base Information

• Chemical Name: deoxybenzoin o-methoxyphenylhydrazone
• CAS No.: 34159-01-8
• Molecular Formula: C₂₁H₂₀N₂O
• Molecular Weight: 316.403
• Mol file: 34159-01-8.mol

Synonyms:deoxybenzoin o-methoxyphenylhydrazone

Chemical Property of deoxybenzoin o-methoxyphenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of deoxybenzoin o-methoxyphenylhydrazone

There total 2 articles about deoxybenzoin o-methoxyphenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl benzyl ketone (451-40-1) + (2-methoxyphenyl)hydrazine (18312-46-4) → deoxybenzoin o-methoxyphenylhydrazone (34159-01-8)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1016/S0040-4020(01)82356-5

Reference yield:

→ deoxybenzoin o-methoxyphenylhydrazone (34159-01-8)

Guidance literature:

o-Methoxy-phenylhydrazin, wss.HCl, Deoxybenzoin, EtOH <Δ>;

Reference yield: 70.0%

deoxybenzoin o-methoxyphenylhydrazone (34159-01-8) → 7-methoxy-2,3-diphenyl-1H-indole (30000-87-4)

Guidance literature:

With phosphorus trichloride; In dichloromethane; for 0.166667h; Ambient temperature;

DOI:10.1016/S0040-4020(01)82356-5

upstream raw materials:

phenyl benzyl ketone

(2-methoxyphenyl)hydrazine

Downstream raw materials:

7-methoxy-2,3-diphenyl-1H-indole