(S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Base Information

Chemical Name:(S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid
CAS No.:1351987-24-0
Molecular Formula:C₁₇H₂₁NO₅
Molecular Weight:319.357
Hs Code.:

Synonyms:(S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Suppliers and Price of (S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

There total 5 articles about (S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1351987-23-9
(S)-benzyl-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl-pentanoate

: 1351987-24-0
(S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; for 24h; under 760.051 Torr;

Reference yield:

: 108-12-3
isopentanoyl chloride

: 1351987-24-0
(S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dmap / dichloromethane / 0.5 h / 0 - 10 °C

2.1: diisopropylamine; n-hexyllithium / hexane; tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 20 °C

With n-hexyllithium; triethylamine; diisopropylamine; trifluoroacetic acid; dmap; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 1351987-24-0
(S)-3-((S)-4-benzyloxazolidin-2-on-3-yl)-carbonyl-4-methyl pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dmap / dichloromethane / 0.5 h / 0 - 10 °C

2.1: diisopropylamine; n-hexyllithium / hexane; tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 20 °C

With n-hexyllithium; triethylamine; diisopropylamine; trifluoroacetic acid; dmap; In tetrahydrofuran; hexane; dichloromethane;