(4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

Base Information

Chemical Name:(4,4-dimethylpent-1-ene-1,1-diyl)dibenzene
CAS No.:66292-25-9
Molecular Formula:C₁₉H₂₂
Molecular Weight:250.384
Hs Code.:

Synonyms:(4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

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Chemical Property of (4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

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Technology Process of (4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

There total 13 articles about (4,4-dimethylpent-1-ene-1,1-diyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 530-48-3
1,1-Diphenylethylene

: 1070-83-3
tert-Butylacetic acid

: 66292-25-9
(4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

Guidance literature:: With potassium phosphate; Co^III(dimethylglyoximate)₂(4-NMe₂-C₅H₄N)Cl; 9-(2-mesityl)-10-methylacridinium perchlorate; In toluene; at 39 - 41 ℃; for 36h; Irradiation; Glovebox; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.8b11218

Reference yield: 41.0%

: 13249-58-6
1-bromo-2,2-diphenylethylene

: 630-17-1
2,2-dimethylpropyl bromide

: 66292-25-9
(4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); tris-(trimethylsilyl)silane; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; sodium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; In 1,2-dimethoxyethane; at 35 ℃; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1039/c8cc08362b

Reference yield: 30.0%

: 10284-47-6
chloro(2,2-dimethylpropyl)mercury

: 67341-86-0
Ph₂CCHHgBr

: 66292-25-9
(4,4-dimethylpent-1-ene-1,1-diyl)dibenzene

Guidance literature:: In dimethyl sulfoxide; Irradiation (UV/VIS); mixt. of substrate and mercurial (5 equiv) is irradiated in nitrogen-purged solvent in Pyrex tube with 350-nm Rayonet photoreactor for 12 h; mixt. is poured into water, extd., extract is washed twice with aq. sodium thiosulfate, dried over anhyd. Na2SO4, concd.; GLC, (1)H-NMR, GCMS;
DOI:10.1021/om00093a020