Technology Process of C44H55F3N6O7
There total 8 articles about C44H55F3N6O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; potassium iodide;
In
N,N-dimethyl-formamide;
at 70 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 85 °C
2: hydrogen / palladium on activated charcoal / methanol / 20 °C
3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 50 °C
4: hydrogen / palladium on activated charcoal / ethyl acetate; methanol / 1 h / 20 °C
5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.5 h / 0 - 20 °C
6: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 70 °C
With
copper(l) iodide; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; L-proline; potassium iodide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 50 °C
2: hydrogen / palladium on activated charcoal / ethyl acetate; methanol / 1 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.5 h / 0 - 20 °C
4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 70 °C
With
hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; potassium iodide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
