dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

Base Information

Chemical Name:dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate
CAS No.:105206-97-1
Molecular Formula:C₂₂H₂₄N₂O₆
Molecular Weight:412.442
Hs Code.:

Synonyms:dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

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Technology Process of dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

There total 4 articles about dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 79-37-8
oxalyl dichloride

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 105206-97-1
dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1016/j.tetasy.2005.01.039

Reference yield: 90.0%

: 79-37-8
oxalyl dichloride

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 105206-97-1
dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jo00376a022

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 105206-97-1
dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: (C₂H₅)3N / CH₂Cl₂

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)98674-X