(2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

Base Information

Chemical Name:(2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol
CAS No.:103747-96-2
Molecular Formula:C₂₀H₂₈N₂O₂
Molecular Weight:328.455
Hs Code.:

Synonyms:(2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

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Chemical Property of (2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

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Technology Process of (2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

There total 5 articles about (2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3182-95-4
L-Phenylalaninol

: 106-93-4
ethylene dibromide

: 103747-96-2
(2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

Guidance literature:: L-Phenylalaninol; ethylene dibromide; at 100 ℃; for 16h;

With sodium hydroxide; water; at 20 ℃;
DOI:10.1016/j.tetasy.2008.10.011

Reference yield: 65.0%

: 105206-97-1
dimethyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate

: 103747-96-2
(2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;
DOI:10.1021/jo00376a022

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 103747-96-2
(2S)-2-[(2-{[(2S)-1-hydroxy-3-phenylpropan-2-yl]amino}ethyl)amino]-3-phenylpropan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine / CH₂Cl₂

2: 65 percent / LiAlH₄ / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00376a022