dimethoxytriphenylphosphorane

Base Information

• Chemical Name: dimethoxytriphenylphosphorane
• CAS No.: 86825-61-8
• Molecular Formula: C₂₀H₂₁O₂P
• Molecular Weight: 324.359
• Mol file: 86825-61-8.mol

Synonyms:dimethoxytriphenylphosphorane

Chemical Property of dimethoxytriphenylphosphorane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of dimethoxytriphenylphosphorane

There total 2 articles about dimethoxytriphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

methanol (67-56-1) + triphenylphosphine (603-35-0) → dimethoxytriphenylphosphorane (86825-61-8)

Guidance literature:

With di-isopropyl azodicarboxylate; In tetrahydrofuran;

DOI:10.1021/jo00087a047

Reference yield:

sodium methylate (124-41-4) + benzyltriphenylphosphonium chloride (1100-88-5) → dimethoxytriphenylphosphorane (86825-61-8)

Guidance literature:

In methanol; dimethyl sulfoxide; at 30 ℃; Further Variations:; Solvents; Temperatures; Reagents; Kinetics;

Reference yield:

dimethoxytriphenylphosphorane (86825-61-8) + trimethyleneglycol (504-63-2) → C22H25O3P (107697-77-8) + C41H42O4P2 (107697-78-9)

Guidance literature:

upstream raw materials:

methanol

triphenylphosphine

sodium methylate

benzyltriphenylphosphonium chloride

Downstream raw materials:

C₂₂H₂₅O₃P

C₄₁H₄₂O₄P₂