2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide

Base Information

Chemical Name:2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide
CAS No.:876048-17-8
Molecular Formula:C₂₀H₁₇N₃O₂S₂
Molecular Weight:395.506
Hs Code.:

Synonyms:2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide

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Chemical Property of 2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide

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Technology Process of 2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide

There total 2 articles about 2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 876048-15-6
2-[1-(4-methylphenylsulphonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yliden] malononitrile

: 876048-17-8
2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide

Guidance literature:: With morpholine; sulfur; In ethanol; Heating;

Reference yield:

: 24310-36-9
1-tosyl-2,3,4,5-tetrahydro-1H-1-benzazepin-5-one

: 876048-17-8
2-amino-6-(4-methylphenylsulphonyl)-5,6-dihydro-4H-benzo[b]thieno[3,2-d]azepin-1-yl cyanide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / Heating

2: 90 percent / sulfur; morpholine / ethanol / Heating

With morpholine; sulfur; triethylamine; In ethanol; 1: Knoevenagel condensation;