2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester
CAS No.:716315-40-1
Molecular Formula:C₂₄H₂₅O₄P
Molecular Weight:408.434
Hs Code.:

Synonyms:2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Suppliers and Price of 2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

There total 4 articles about 2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3282-30-2
pivaloyl chloride

: 120726-60-5
(2-hydroxy-5-methoxyphenyl)diphenylphosphine oxide

: 716315-40-1
2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2004.03.073

Reference yield:

: 34253-15-1
4-methoxy-o-phenyl phenyl(phenyl)phosphinate

: 716315-40-1
2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / LDA / tetrahydrofuran / 6 h / -60 °C

2: 99 percent / Et₃N / CH₂Cl₂

With triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2004.03.073

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 716315-40-1
2,2-dimethyl-propionic acid 2-(diphenyl-phosphinoyl)-4-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N / CH₂Cl₂ / 12 h / 20 °C

1.2: 99 percent / H₂O₂

2.1: 74 percent / LDA / tetrahydrofuran / 6 h / -60 °C

3.1: 99 percent / Et₃N / CH₂Cl₂

With triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2004.03.073