1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Base Information

Chemical Name:1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester
CAS No.:467443-26-1
Molecular Formula:C₂₃H₂₁ClN₂O₅
Molecular Weight:440.883
Hs Code.:

Synonyms:1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Suppliers and Price of 1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

There total 4 articles about 1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 79-37-8
oxalyl dichloride

: 467443-18-1
1-[3-(4-chloro-phenyl)-ureido]-cyclohexanecarboxylic acid benzyl ester

: 467443-26-1
1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.3797/scipharm.aut-01-204

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 467443-26-1
1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / toluene / 1 h / Heating

2: 60 percent / CHCl₃ / 3 h / 20 °C

3: 53 percent / tetrahydrofuran / 3 h / 0 - 20 °C

With sodium azide; In tetrahydrofuran; chloroform; toluene;
DOI:10.3797/scipharm.aut-01-204

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 467443-26-1
1-[3-(4-chloro-phenyl)-2,4,5-trioxo-imidazolidin-1-yl]-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: sodium azide / toluene / 1 h / Heating

3: 60 percent / CHCl₃ / 3 h / 20 °C

4: 53 percent / tetrahydrofuran / 3 h / 0 - 20 °C

With thionyl chloride; sodium azide; In tetrahydrofuran; chloroform; toluene;
DOI:10.3797/scipharm.aut-01-204