Benzeneethanol, 2,6-difluoro- (9CI)

Base Information

• Chemical Name: Benzeneethanol, 2,6-difluoro- (9CI)
• CAS No.: 168766-16-3
• Molecular Formula: C8H8 F2 O
• Molecular Weight: 158.148
• Mol file: 168766-16-3.mol

Synonyms:2-(2,6-Difluorophenyl)ethanol

Chemical Property of Benzeneethanol, 2,6-difluoro- (9CI)

Chemical Property:

• Boiling Point: 201.5±25.0 °C(Predicted)
• PKA: 14.49±0.10(Predicted)
• PSA: 20.23000
• Density: 1.233±0.06 g/cm3(Predicted)
• LogP: 1.49960
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

2-(2,6-difluorophenyl)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneethanol, 2,6-difluoro- (9CI)

There total 4 articles about Benzeneethanol, 2,6-difluoro- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

→ 2-(2,6-difluorophenyl)ethanol (168766-16-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

(2,6-difluorophenyl)acetic acid methyl ester (872046-08-7) → 2-(2,6-difluorophenyl)ethanol (168766-16-3)

Guidance literature:

(2,6-difluorophenyl)acetic acid methyl ester; With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 2h;

With sodium hydroxide; water; In diethyl ether;

Reference yield:

(2,6-difluorophenyl)acetic acid ethyl ester (680217-71-4) → 2-(2,6-difluorophenyl)ethanol (168766-16-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1021/jm200385u

upstream raw materials:

(2,6-difluorophenyl)acetic acid methyl ester

(2,6-difluorophenyl)acetic acid ethyl ester

2,6-difluorophenylacetic acid

Downstream raw materials:

2-(2,6-difluoro-3-nitrophenyl)ethyl acetate

2-[2-({2-[(tert-butoxycarbonyl)amino]ethyl}amino)-6-fluoro-3-nitrophenyl]ethyl acetate

tert-butyl [2-(2-phenyl-7,8-dihydro-1H-furo[3,2-e]benzimidazol-1-yl)ethyl]carbamate

N-[2-(2-phenyl-7,8-dihydro-1H-furo[3,2-e]benzimidazol-1-yl)ethyl]acetamide

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