((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Base Information

Chemical Name:((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate
CAS No.:1563184-61-1
Molecular Formula:C₁₇H₂₇N₃O₁₂S₃
Molecular Weight:561.612
Hs Code.:

Synonyms:((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

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Chemical Property of ((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

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Technology Process of ((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

There total 6 articles about ((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 109-83-1
(2-hydroxyethyl)(methyl)amine

: 1563184-60-0
5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid

: 1563184-61-1
((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Guidance literature:: 5-(bis(2-((methylsulfonyl)oxy)ethyl)amino)-4-(methylsulfonyl)-2-nitrobenzoic acid; With oxalyl dichloride; magnesium oxide; N,N-dimethyl-formamide; In dichloromethane; acetonitrile; at 0 - 20 ℃; for 4h;

(2-hydroxyethyl)(methyl)amine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 0.333333h;

Reference yield:

: 34036-07-2
3,4 difluorobenzaldehyde

: 1563184-61-1
((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Guidance literature:: Multi-step reaction with 8 steps

1.1: dimethyl sulfoxide / 3 h / 75 °C / Inert atmosphere

2.1: sodium dihydrogen phosphate monohydrate; dihydrogen peroxide; sodium chlorite; hydrogenchloride / acetonitrile; water / 0 - 20 °C

3.1: sulfuric acid; nitric acid / 4 h / 45 °C

4.1: perchloric acid / acetonitrile / 48 h / 20 °C

5.1: dimethyl sulfoxide / 2 h / 20 °C

6.1: triethylamine / dichloromethane / 0.33 h / 0 °C

7.1: trifluoroacetic acid / dichloromethane / 5 - 20 °C

8.1: N,N-dimethyl-formamide; magnesium oxide; oxalyl dichloride / dichloromethane; acetonitrile / 4 h / 0 - 20 °C

8.2: 0.33 h / 0 - 20 °C

With hydrogenchloride; sodium chlorite; perchloric acid; sodium dihydrogen phosphate monohydrate; oxalyl dichloride; sulfuric acid; dihydrogen peroxide; nitric acid; magnesium oxide; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In dichloromethane; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 185945-88-4
3-fluoro-4-(methylsulfonyl)benzoic acid

: 1563184-61-1
((5-((2-hydroxyethyl)(methyl)carbamoyl)-2-(methylsulfonyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl) dimethanesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid; nitric acid / 4 h / 45 °C

2.1: perchloric acid / acetonitrile / 48 h / 20 °C

3.1: dimethyl sulfoxide / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 0.33 h / 0 °C

5.1: trifluoroacetic acid / dichloromethane / 5 - 20 °C

6.1: N,N-dimethyl-formamide; magnesium oxide; oxalyl dichloride / dichloromethane; acetonitrile / 4 h / 0 - 20 °C

6.2: 0.33 h / 0 - 20 °C

With perchloric acid; oxalyl dichloride; sulfuric acid; nitric acid; magnesium oxide; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; acetonitrile;