5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole
CAS No.:934503-47-6
Molecular Formula:C₄₄H₈₀N₄OS
Molecular Weight:713.211
Hs Code.:

Synonyms:5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

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Chemical Property of 5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

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Technology Process of 5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

There total 23 articles about 5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 934503-45-4
(16R,17R)-1-bromo-16-methoxy-17-methylpentatriacontane

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 934503-47-6
5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 18h;
DOI:10.1016/j.tet.2007.01.007

Reference yield:

: 943962-72-9
2,2-dimethyl-propionic acid 8-bromooctyl ester

: 934503-47-6
5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / potassium carbonate / acetone / 16 h / 20 °C

2: 89 percent / ammonium molybdate(VI) tetrahydrate; aq. hydrogen peroxide / tetrahydrofuran; various solvent(s) / 2 h / 20 °C

3: 91 percent / lithium hexamethyldisilazide / tetrahydrofuran / 16 h / 20 °C

4: 93 percent / hydrogen / palladium on charcoal / ethanol

5: 98 percent / potassium hydroxide / methanol; tetrahydrofuran / 3 h / 40 °C

6: 85 percent / N-bromosuccinimide; triphenylphosphine / CH₂Cl₂ / 1 h / 20 °C

7: 91 percent / potassium carbonate / acetone / 18 h / 20 °C

With potassium hydroxide; N-Bromosuccinimide; ammonium molybdate tetrahydrate; hydrogen; dihydrogen peroxide; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone; 3: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2007.01.007

Reference yield:

: 934502-91-7
2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

: 934503-47-6
5-((16R,17R)-16-methoxy-17-methylpentatriacontyl-1-sulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / lithium hexamethyldisilazide / tetrahydrofuran / 16 h / 20 °C

2: 93 percent / hydrogen / palladium on charcoal / ethanol

3: 98 percent / potassium hydroxide / methanol; tetrahydrofuran / 3 h / 40 °C

4: 85 percent / N-bromosuccinimide; triphenylphosphine / CH₂Cl₂ / 1 h / 20 °C

5: 91 percent / potassium carbonate / acetone / 18 h / 20 °C

With potassium hydroxide; N-Bromosuccinimide; hydrogen; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone; 1: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2007.01.007