Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside

Base Information

Chemical Name:Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside
CAS No.:105930-93-6
Molecular Formula:C₄₁H₇₀N₂O₉Si₃
Molecular Weight:819.271
Hs Code.:

Synonyms:Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside

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Chemical Property of Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside

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Technology Process of Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside

There total 7 articles about Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67-56-1
methanol

: 105930-88-9
(4aS,6S,7S,8S,8aS)-3-Benzyloxy-7,8-bis-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-dimethyl-silanyloxymethyl)-6,7,8,8a-tetrahydro-4aH-pyrano[3,2-e][1,3,4]oxadiazine-1-carboxylic acid benzyl ester

: 105930-93-6
C₄₁H₇₀N₂O₉Si₃

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 0.0333333h; Ambient temperature;
DOI:10.1016/S0040-4039(00)99150-0

Reference yield: 88.0%

: 67-56-1
methanol

: 105930-88-9
<4aR-(4aα,6α,8α,8aα)>-7,8-Bis<<(1,1-dimethylethyl)dimethylsilyl>oxy>-6-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-4a,7,8,8a-tetrahydro-3-(phenylmethoxy)-1H,6H-pyrano<3,2-e><1,3,4>oxadiazine-1-carboxylic acid phenylmethyl ester

: 105930-93-6
Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; Ambient temperature;
DOI:10.1021/ja00190a037

Reference yield:

: 79999-47-6
tri-O-(tert-butyldimethylsilyl)-D-glucal

: 105930-93-6
Methyl 2-<1,2-bis<(phenylmethoxy)carbonyl>hydrazino>-2-deoxy-3,4,6-tris-O-<(1,1-dimethylethyl)dimethylsilyl>-Sb-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / cyclohexane; CH₂Cl₂ / Irradiation

2: 88 percent / p-TsOH*H₂O

With toluene-4-sulfonic acid; In dichloromethane; cyclohexane;
DOI:10.1021/ja00235a050