methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

Base Information

Chemical Name:methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate
CAS No.:1240612-98-9
Molecular Formula:C₁₆H₂₀F₃NO₄
Molecular Weight:347.334
Hs Code.:

Synonyms:methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

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Chemical Property of methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

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Technology Process of methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

There total 2 articles about methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 142995-31-1
(2S)-2-[(tert-butoxycarbonyl)amino]-3-[3-(trifluoromethyl)phenyl]propanoic acid

: 74-88-4
methyl iodide

: 1240612-98-9
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol1015674

Reference yield: 48.0%

: 401-81-0
m-trifluoromethylphenyl iodide

: 93267-04-0,170848-34-7,889670-02-4
N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester

: 915040-50-5
(2S,5S)-2,5-bis-tert-butoxycarbonylaminohexane-1,6-dioic acid dimethyl ester

: 1240612-98-9
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; dichloro bis((p-dimethylaminophenyl)-?-di-tert-butylphosphine)palladium(II); zinc; In water; at 65 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo102334c

Reference yield: 84.0%

: 1240612-98-9
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(trifluoromethyl)phenyl)propanoate

: 73183-34-3
bis(pinacol)diborane

: 1240613-05-1
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl)propanoate

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In hexane; at 60 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol1015674