1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine

Base Information

• Chemical Name: 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine
• CAS No.: 179481-95-9
• Molecular Formula: C₂₁H₁₈N₄O₉
• Molecular Weight: 470.395

Synonyms:1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine

Chemical Property of 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine

Chemical Property:

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Technology Process of 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine

There total 3 articles about 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-Nitrophenyl chloroformate (7693-46-1) + 1,6-dihydro-5-methoxycarbonyl-2-methoxy-4-methyl-6-(4-nitrophenyl)pyrimidine (179481-94-8,179481-98-2,179481-99-3) → 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine (179481-95-9)

Guidance literature:

With dmap; In dichloromethane;

DOI:10.1016/S0960-894X(99)00653-8

Reference yield: 89.0%

PYRIMIDINE (289-95-2,25247-63-6) + 1,6-Dihydro-5-methoxycarbonyl-2-methoxy-4-methyl-6-(4-nitro-phenyl)-pyrimidine (179481-94-8,179481-98-2,179481-99-3) + 4-Nitrophenyl chloroformate (7693-46-1) → 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine (179481-95-9)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield: 89.0%

PYRIMIDINE (289-95-2,25247-63-6) + 1,6-Dihydro-5-methoxycarbonyl-2-methoxy-4-methyl-6-(4-nitro-phenyl)-pyrimidine (179481-94-8,179481-98-2,179481-99-3) + dichloromethane (75-09-2) + 4-Nitrophenyl chloroformate (7693-46-1) → 1,6-dihydro-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)-1-[(4-nitrophenyloxy)carbonyl]pyrimidine (179481-95-9)

Guidance literature:

With sodium hydrogencarbonate; In water;

upstream raw materials:

4-Nitrophenyl chloroformate

1,6-dihydro-5-methoxycarbonyl-2-methoxy-4-methyl-6-(4-nitrophenyl)pyrimidine

PYRIMIDINE

1,6-Dihydro-5-methoxycarbonyl-2-methoxy-4-methyl-6-(4-nitro-phenyl)-pyrimidine

Downstream raw materials:

1,6-dihydro-1-{N-[3-(4,4-diphenylpiperidin-1-yl)propyl]carboxamido}-2-methoxy-5-methoxycarbonyl-4-methyl-6-(4-nitrophenyl)pyrimidine

2-methoxy-1-[3-(4-methoxycarbonyl-4-phenyl-piperidin-1-yl)-propylcarbamoyl]-4-methyl-6-(4-nitro-phenyl)-1,6-dihydro-pyrimidine-5-carboxylic acid methyl ester

4-(4-nitro-phenyl)-2,5-dioxo-1,2,5,7-tetrahydro-4H-furo[3,4-d]pyrimidine-3-carboxylic acid 4-nitro-phenyl ester

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