2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

Base Information

Chemical Name:2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate
CAS No.:1437779-66-2
Molecular Formula:C₁₉H₁₃BrCl₂F₃NO₃
Molecular Weight:511.122
Hs Code.:

Synonyms:2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

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Chemical Property of 2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

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Technology Process of 2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

There total 9 articles about 2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1437779-65-1
3-(4-bromo-3-(bromomethyl)phenyl)-5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

: 127-09-3
sodium acetate

: 1437779-66-2
2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

Guidance literature:: With acetic acid; for 16h; Reflux;

Reference yield:

: 67492-50-6
(3,5-dichlorophenyl)boronic acid

: 1437779-66-2
2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / tetrahydrofuran; water / 4 h / 70 °C / Sealed tube

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.67 h / 40 °C

2.2: 20 h / 0 - 20 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 3.5 h / Reflux

4.1: acetic acid / 16 h / Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-chloro-succinimide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; acetic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 149104-89-2
4-bromo-3-methylbenzylalcohol

: 1437779-66-2
2-bromo-5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: manganese(IV) oxide / dichloromethane / 12 h / 20 °C

2.1: hydroxylamine hydrochloride; triethylamine / ethanol / 2 h / Reflux

3.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.67 h / 40 °C

3.2: 20 h / 0 - 20 °C

4.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 3.5 h / Reflux

5.1: acetic acid / 16 h / Reflux

With manganese(IV) oxide; N-chloro-succinimide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydroxylamine hydrochloride; acetic acid; triethylamine; In ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;