IsPH(CH₂)3PHIs

Base Information

Chemical Name:IsPH(CH₂)3PHIs
CAS No.:1221169-71-6
Molecular Formula:C₃₃H₅₄P₂
Molecular Weight:512.739
Hs Code.:

Synonyms:IsPH(CH₂)3PHIs

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Chemical Property of IsPH(CH₂)3PHIs

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Technology Process of IsPH(CH₂)3PHIs

There total 2 articles about IsPH(CH₂)3PHIs which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 112438-22-9
(2,4,6-triisopropylphenyl)phosphine

: 109-64-8
1,3-dibromo-propane

: 1221169-71-6
IsPH(CH₂)3PHIs

Guidance literature:: (2,4,6-triisopropylphenyl)phosphine; With potassium carbonate; potassium hydroxide; In 1,3,5-triisopropyl benzene; dimethyl sulfoxide; at 20 ℃; for 30h; Inert atmosphere;

1,3-dibromo-propane; In 1,3,5-triisopropyl benzene; dimethyl sulfoxide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ic100219j

Reference yield: 51.0%

: C₃₃H₅₆B₂P₂

: 1221169-71-6
IsPH(CH₂)3PHIs

Guidance literature:: With piperazinomethylpolystyrene; In toluene; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ic100219j

Reference yield: 91.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 75-09-2
dichloromethane

: 1221169-71-6
IsPH(CH₂)3PHIs

: [(2,4,6-(i-Pr)3C₆H₂)HP(CH₂)3PH(2,4,6-(i-Pr)3C₆H₂)(AuCl)2]*0.75CH₂Cl₂

Guidance literature:: In dichloromethane; (N2); std. Schlenk technique; soln. of P ligand in CH2Cl2 was added to soln. of Au complex (2 equiv.) in CH2Cl2; stirred for 30 min; evapd. (vac.); recrystd. (CH2Cl2); elem. anal.;
DOI:10.1021/ic100219j