threo-3-Hydroxy-2,3-diphenylpropionic acid

Base Information

Chemical Name:threo-3-Hydroxy-2,3-diphenylpropionic acid
CAS No.:4603-32-1
Molecular Formula:C₁₅H₁₄O₃
Molecular Weight:242.274
Hs Code.:

Synonyms:threo-3-Hydroxy-2,3-diphenylpropionic acid

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Chemical Property of threo-3-Hydroxy-2,3-diphenylpropionic acid

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Technology Process of threo-3-Hydroxy-2,3-diphenylpropionic acid

There total 17 articles about threo-3-Hydroxy-2,3-diphenylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 15082-44-7,66730-64-1
dilithium phenyl acetic acid

: 100-52-7
benzaldehyde

: 4603-32-1,4603-33-2,5449-26-3,52515-81-8,58769-50-9,58769-51-0,93059-95-1
α-benzenessigsaeure

Guidance literature:: With optically active alkoxide base; In diethyl ether; at -110 ℃; for 0.5h;
DOI:10.1016/0040-4020(84)80003-4

Reference yield: 69.0%

: 114-70-5
sodium phenylacetate

: 100-52-7
benzaldehyde

: 4603-33-2
erythro-3-Hydroxy-2,3-diphenylpropionic acid

: 4603-32-1
threo-3-Hydroxy-2,3-diphenylpropionic acid

Guidance literature:: sodium phenylacetate; With isopropyl chloride; magnesium; In tetrahydrofuran; at 0 ℃;

benzaldehyde; In tetrahydrofuran; at 0 ℃; for 4h; Reflux;
DOI:10.5560/ZNB.2013-2271

Reference yield:

: 31491-21-1
2-phenyl-1,1-bis(trimethylsilyloxy)ethene

: 100-52-7
benzaldehyde

: 4603-32-1,4603-33-2,5449-26-3,52515-81-8,58769-50-9,58769-51-0,93059-95-1
(2RS,3RS)-3-hydroxy-2,3-diphenyl-propionic acid

: 4603-32-1,4603-33-2,5449-26-3,52515-81-8,58769-50-9,58769-51-0,93059-95-1
α-benzenessigsaeure

Guidance literature:: titanium tetrachloride; In dichloromethane; at -50 ℃; for 0.0833333h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(01)91225-0