1-<(tert-Butoxycarbonyl)amino>-5-pentane

Base Information

Chemical Name:1-<(tert-Butoxycarbonyl)amino>-5-pentane
CAS No.:83948-51-0
Molecular Formula:C₁₉H₃₀N₂O₄
Molecular Weight:350.458
Hs Code.:

1-<(tert-Butoxycarbonyl)amino>-5-<acetyl(benzyloxy)amino>pentane

Synonyms:1-<(tert-Butoxycarbonyl)amino>-5-pentane

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Chemical Property of 1-<(tert-Butoxycarbonyl)amino>-5-pentane

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Technology Process of 1-<(tert-Butoxycarbonyl)amino>-5-pentane

There total 5 articles about 1-<(tert-Butoxycarbonyl)amino>-5-pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 94136-60-4
5-<(tert-butoxycarbonyl)amino>pentanal O-benzyloxime

: 94427-31-3
2-Methoxy-4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenol; hydrochloride

: 83948-51-0
1-<(tert-Butoxycarbonyl)amino>-5-pentane

Guidance literature:: With sodium cyanoborohydride; In acetic acid; for 1.5h; Ambient temperature;
DOI:10.1021/jm00381a010

Reference yield: 62.0%

: 4797-81-3
N-benzyloxyacetamide

: 83948-54-3
tert-butyl (5-bromopentyl)carbamate

: 83948-56-5
N-Benzyloxy-acetimidic acid 5-tert-butoxycarbonylamino-pentyl ester

: 83948-51-0
1-<(tert-Butoxycarbonyl)amino>-5-pentane

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; for 24h; Heating;
DOI:10.1021/jo00149a005

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 83948-51-0
1-<(tert-Butoxycarbonyl)amino>-5-pentane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / acetonitrile / 24 h / Ambient temperature

2: 78 percent / PPh₃, CBr₄ / tetrahydrofuran / Ambient temperature; 1.) 2 h, 2.) stirring overnight

3: 62 percent / KI, K₂CO₃ / acetone / 24 h / Heating

With carbon tetrabromide; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; acetone; acetonitrile;
DOI:10.1021/jo00149a005