2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

Base Information

Chemical Name:2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole
CAS No.:75817-46-8
Molecular Formula:C₁₆H₂₅NO₂Si
Molecular Weight:291.466
Hs Code.:

Synonyms:2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

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Chemical Property of 2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

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Technology Process of 2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

There total 2 articles about 2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 75-77-4
chloro-trimethyl-silane

: 75817-44-6
2-(2-methyl-4-methoxyphenyl)4,4-dimethyl-2-oxazoline

: 75817-46-8
2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

Guidance literature:: With n-butyllithium;
DOI:10.1021/ja00542a055

Reference yield:

: 53416-46-9
2-(4-methoxyphenyl)-4,4-dimethyl-2-oxazoline

: 75817-46-8
2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / n-BuLi / diethyl ether

2: 92 percent / n-BuLi

With n-butyllithium; In diethyl ether;
DOI:10.1021/ja00542a055

Reference yield:

: 75817-46-8
2-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

: 75817-49-1
(2S,3S)-2-[(E)-3-(4-Methoxy-2-trimethylsilanylmethyl-phenyl)-allyl]-2-methyl-3-vinyl-cyclopentanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) methyl iodide, 2.) NaBH₄ / 1.) nitromethane, 2.) ethanol

2: 95 percent

3: zinc bromide / CH₂Cl₂ / -78 - -20 °C

With sodium tetrahydroborate; zinc dibromide; methyl iodide; In dichloromethane;
DOI:10.1021/ja00542a055