N'-(2-bromo-1-phenylethylidene)acetohydrazide

Base Information

• Chemical Name: N'-(2-bromo-1-phenylethylidene)acetohydrazide
• CAS No.: 808798-00-7
• Molecular Formula: C₁₀H₁₁BrN₂O
• Molecular Weight: 255.114
• Mol file: 808798-00-7.mol

Synonyms:N'-(2-bromo-1-phenylethylidene)acetohydrazide

Chemical Property of N'-(2-bromo-1-phenylethylidene)acetohydrazide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N'-(2-bromo-1-phenylethylidene)acetohydrazide

There total 1 articles about N'-(2-bromo-1-phenylethylidene)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

acetic acid hydrazide (1068-57-1) + α-bromoacetophenone (70-11-1) → N'-(2-bromo-1-phenylethylidene)acetohydrazide (808798-00-7)

Guidance literature:

With hydrogenchloride; In methanol; water; at 0 ℃; for 3h;

DOI:10.1039/c3cc43888k

Reference yield: 99.0%

di-isopropyl azodicarboxylate (2446-83-5) + N'-(2-bromo-1-phenylethylidene)acetohydrazide (808798-00-7) → diisopropyl 3-acetyl-5-phenyl-1,2,3,4-tetrazine-1,2(3H,6H)-dicarboxylate

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 18h; Reagent/catalyst; Solvent;

DOI:10.1039/c6ra01359g

Reference yield: 96.0%

N'-(2-bromo-1-phenylethylidene)acetohydrazide (808798-00-7) → 1-(3,6-diphenyl-5,6-dihydropyridazin-1(4H)-yl)ethan-1-one

Guidance literature:

With potassium carbonate; cesium fluoride; In acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.orglett.6b01551

upstream raw materials:

acetic acid hydrazide

α-bromoacetophenone

Downstream raw materials:

C₂₆H₂₄N₄O₂

C₂₇H₂₆N₄O₂

C₂₆H₂₃ClN₄O₂

C₂₁H₂₂N₄O₂