C₆₅H₇₁N₆O₁₅P

Base Information

Chemical Name:C₆₅H₇₁N₆O₁₅P
CAS No.:130887-31-9
Molecular Formula:C₆₅H₇₁N₆O₁₅P
Molecular Weight:1207.28
Hs Code.:

C<sub>65</sub>H<sub>71</sub>N<sub>6</sub>O<sub>15</sub>P

Synonyms:C₆₅H₇₁N₆O₁₅P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₅H₇₁N₆O₁₅P

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Technology Process of C₆₅H₇₁N₆O₁₅P

There total 11 articles about C₆₅H₇₁N₆O₁₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 130867-68-4
C₅₆H₅₄N₄O₁₄

: 130887-31-9
C₆₅H₇₁N₆O₁₅P

Guidance literature:: With 1H-tetrazole;

Reference yield:

: 130867-57-1
5’-O-dimethoxytrityl-3’-O-methoxyacetylthymidine

: 130887-31-9
C₆₅H₇₁N₆O₁₅P

Guidance literature:: Multi-step reaction with 5 steps

1: N,N-diisopropylethylamine (DIPEA) / pyridine / 1 h / Ambient temperature

2: 85 percent / 90percent aq. acetic acid / 0.5 h / 50 °C

3: 33 percent / molecular sieves (4 Angstroem) / 1,2-dichloro-ethane / 72 h / Ambient temperature

4: 96 percent / potassium-tert.-butoxide / CH₂Cl₂; methanol / 0.25 h / Ambient temperature

5: 82 percent / N,N-diisopropylethylamine (DIPEA) / 1,2-dichloro-ethane / 0.17 h / Ambient temperature

With 4 A molecular sieve; potassium tert-butylate; acetic acid; N-ethyl-N,N-diisopropylamine; In pyridine; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)86429-2

Reference yield:

: 102573-69-3
5'-O-(4-4'-dimethoxytrityl)-N³-benzoyl thymidine

: 130887-31-9
C₆₅H₇₁N₆O₁₅P

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / benzoyl peroxide, 2,6-lutidine / acetonitrile / 2 h / Ambient temperature

2: 33 percent / molecular sieves (4 Angstroem) / 1,2-dichloro-ethane / 72 h / Ambient temperature

3: 96 percent / potassium-tert.-butoxide / CH₂Cl₂; methanol / 0.25 h / Ambient temperature

4: 82 percent / N,N-diisopropylethylamine (DIPEA) / 1,2-dichloro-ethane / 0.17 h / Ambient temperature

With 2,6-dimethylpyridine; 4 A molecular sieve; potassium tert-butylate; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In methanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/S0040-4020(01)86429-2