tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate

Base Information

• Chemical Name: tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate
• CAS No.: 1356864-75-9
• Molecular Formula: C₁₅H₂₂N₂O₇S
• Molecular Weight: 374.415

Synonyms:tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate

Chemical Property of tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate

Chemical Property:

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Technology Process of tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate

There total 1 articles about tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 3-bromopropionate (55666-43-8) + N-(2-hydroxy-ethyl)-2-nitro-benzenesulfonamide (18226-11-4) → tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate (1356864-75-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; Inert atmosphere;

Reference yield:

tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate (1356864-75-9) + methanesulfonyl chloride (124-63-0) → tert-butyl 3-[(2-methanesulfonyloxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate (1356864-74-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -5 - 20 ℃; for 2h;

Reference yield:

tert-butyl 3-[(2-hydroxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate (1356864-75-9) → tert-butyl 3-[(2-methanesulfonyloxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate (1356864-74-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In water;

upstream raw materials:

tert-butyl 3-bromopropionate

N-(2-hydroxy-ethyl)-2-nitro-benzenesulfonamide

Downstream raw materials:

tert-butyl 3-[(2-methanesulfonyloxy-ethyl)-(2-nitro-benzenesulfonyl)-amino]-propionate

methyl 3-[[2-(2,6-bis-hydroxymethyl-pyridin-4-yloxy)-ethyl]-(2-nitro-benzenesulfonyl)-amino]-propanoate

tert-butyl 3-[[2-(2,6-bis-hydroxymethyl-pyridin-4-yloxy)-ethyl]-(2-nitro-benzenesulfonyl)-amino]-propanoate

diethyl 4-{2-[(2-tert-butoxycarbonyl-ethyl)-(2-nitro-benzenesulfonyl)-amino]-ethoxy}-pyridine-2,6-dicarboxylate

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