Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

Base Information

Chemical Name:Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene
CAS No.:124337-86-6
Molecular Formula:C₁₂H₂₂OSi
Molecular Weight:210.392
Hs Code.:

Δ<sup>1.6</sup>-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

Synonyms:Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

Chemical Property:

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Technology Process of Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

There total 1 articles about Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 68269-56-7,54735-44-3
3-methyl-3-vinylcyclohexan-1-one

: 102308-02-1
Δ^1.2-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

: 124337-86-6
Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -73 ℃; for 0.0833333h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(01)96005-3

Reference yield: 72.0%

: 124337-86-6
Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

: 124337-85-5
α,α-dimethyl-1-(p-toluenesulfonyl)-1H-indole-4-methanol

: 124337-87-7
5-Methyl-2-{1-methyl-1-[1-(toluene-4-sulfonyl)-1H-indol-4-yl]-ethyl}-5-vinyl-cyclohexanone

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -78 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.09.086

Reference yield:

: 102308-02-1
Δ^1.2-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

: 124337-86-6
Δ^1.6-1-triemthylsilyloxy-3-methyl-3-vinylcyclohexene

: 124337-85-5
α,α-dimethyl-1-(p-toluenesulfonyl)-1H-indole-4-methanol

: 124337-90-2
7,10,10-Trimethyl-3-(toluene-4-sulfonyl)-7-vinyl-3,6,7,8,9,10-hexahydro-indeno[2,1-e]indole

: 124337-88-8
3-Methyl-2-{1-methyl-1-[1-(toluene-4-sulfonyl)-1H-indol-4-yl]-ethyl}-3-vinyl-cyclohexanone

: 124337-89-9
2,6,7,8,9,10-hexahydro-6,6,9-trimethyl-2-p-toluenesulfonyl-9-vinylnaphth<1.2.3-cd>indole

Guidance literature:: With boron trifluoride diethyl etherate; tin(IV) chloride; Yield given. Multistep reaction. Yields of byproduct given; 1) CH₂Cl₂, -78 deg C, 10 min; 2) CH₂Cl₂, 18 deg C, 1.5 h;
DOI:10.1016/S0040-4039(00)99587-X