(1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Base Information

Chemical Name:(1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide
CAS No.:171889-30-8
Molecular Formula:C₂₃H₂₈N₄OSe
Molecular Weight:455.462
Hs Code.:

Synonyms:(1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

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Chemical Property of (1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

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Technology Process of (1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

There total 6 articles about (1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 23974-72-3
sodium phenylselenide

: 171889-29-5
(1S,2R)-1-phenyl-2-[(S)-1-azido-3-tosyloxypropyl]-N,N-diethylcyclopropanecarboxamide

: 171889-30-8
(1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Guidance literature:: In ethanol; for 15h; Ambient temperature;
DOI:10.1021/jm960495w

Reference yield:

: 171889-34-2
(1S,2R)-2-((S)-1,3-Dihydroxy-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

: 171889-30-8
(1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / pyridine / 1.5 h / 0 °C

2: 91 percent / NaN₃, Ph₃P, CBr₄ / dimethylformamide / 3 h / Ambient temperature

3: 99 percent / MeONa, MeOH / 15 h / Ambient temperature

4: 99 percent / Et₃N, DMAP / CH₂Cl₂ / 15 h / Ambient temperature

5: 85 percent / ethanol / 15 h / Ambient temperature

With pyridine; methanol; dmap; sodium azide; carbon tetrabromide; sodium methylate; triethylamine; triphenylphosphine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm960495w

Reference yield:

: 171889-28-4
(1S,2R)-1-phenyl-2-[(S)-1-azido-3-hydroxypropyl]-N,N-diethylcyclopropanecarboxamide

: 171889-30-8
(1S,2R)-2-((S)-1-Azido-3-phenylselanyl-propyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N, DMAP / CH₂Cl₂ / 15 h / Ambient temperature

2: 85 percent / ethanol / 15 h / Ambient temperature

With dmap; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm960495w