1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

Base Information

Chemical Name:1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole
CAS No.:155261-38-4
Molecular Formula:C₂₀H₁₉N₃O₂
Molecular Weight:333.39
Hs Code.:

Synonyms:1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

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Chemical Property of 1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

Chemical Property:

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Technology Process of 1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

There total 3 articles about 1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-98-6
2-Picolinic acid

: 155261-38-4
1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 2 h / Heating

2: Et₃N / tetrahydrofuran / Ambient temperature

3: 1.) ZnCl₂, 2.) 10percent aq. NH₃ / 1.) Et₂O, overnight

With ammonium hydroxide; thionyl chloride; triethylamine; zinc(II) chloride; In tetrahydrofuran;
DOI:10.1021/jo00086a028

Reference yield:

: 29745-44-6
pyridine-2-carbonyl chloride

: 155261-38-4
1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / Ambient temperature

2: 1.) ZnCl₂, 2.) 10percent aq. NH₃ / 1.) Et₂O, overnight

With ammonium hydroxide; triethylamine; zinc(II) chloride; In tetrahydrofuran;
DOI:10.1021/jo00086a028

Reference yield:

: 10198-84-2
2-Picolinoylcyclohexanone

: 4510-12-7
methyl 4-hydrazinobenzoate

: 155261-38-4
1-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

: 2-<4-(Methoxycarbonyl)phenyl>-3-(pyridin-2-yl)-4,5,6,7-tetrahydroindazole

Guidance literature:: With ammonium hydroxide; zinc(II) chloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) Et₂O, overnight;
DOI:10.1021/jo00086a028