Technology Process of 2-methyl-5-(2,3-dimethylphenyl)pentan-2-ol
There total 5 articles about 2-methyl-5-(2,3-dimethylphenyl)pentan-2-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) AlCl3, 2.) K2CO3 / 1.) nitrobenzene a) 3 h, ice-bath temperature raising to 30 deg C, b) 3 h, 30 - 40 deg C, 2.) acetone, 12 h, reflux
2: 76 percent / anhydrous AlCl3 / benzene / 1.) 8 h, 65 deg C, 2.) overnight, room temperature
3: 79 percent / HCl, activated zinc dust / diethyl ether / 1.) during addition, 5 deg C, 2.) 3 h, 0 deg C
4: 1.) Mg / 1.) ether, 2.) a) room temperature, b) 1 h, reflux
With
hydrogenchloride; aluminium trichloride; potassium carbonate; magnesium; zinc;
In
diethyl ether; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 79 percent / HCl, activated zinc dust / diethyl ether / 1.) during addition, 5 deg C, 2.) 3 h, 0 deg C
2: 1.) Mg / 1.) ether, 2.) a) room temperature, b) 1 h, reflux
With
hydrogenchloride; magnesium; zinc;
In
diethyl ether;
