tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

Base Information

Chemical Name:tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate
CAS No.:1263265-94-6
Molecular Formula:C₃₂H₄₇N₃O₅S
Molecular Weight:585.808
Hs Code.:

Synonyms:tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

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Chemical Property of tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

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Technology Process of tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

There total 4 articles about tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1263265-93-5
(9-(3-(2-hydroxyethyl)phenethyl)-1-oxa-4,9-diazaspiro[5.5]undecan-4-yl)(2-isopropylthiazol-4-yl)methanone

: 1263265-94-6
tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In water; acetonitrile; at 20 ℃; for 1h; Product distribution / selectivity;

Reference yield:

: 46133-05-5
1,3-Bis(2'-hydroxyethyl)benzene

: 1263265-94-6
tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide / toluene; water / 38 h / 87 °C / Reflux

2: potassium carbonate / acetonitrile; water / 66 h / 20 - 60 °C

3: N-benzyl-trimethylammonium hydroxide / acetonitrile; water / 1 h / 20 °C

With hydrogen bromide; N-benzyl-trimethylammonium hydroxide; potassium carbonate; In water; toluene; acetonitrile;

Reference yield:

: 19806-17-8
1,3-benzenediacetic acid

: 1263265-94-6
tert-butyl 3-(3-(2-(4-(2-isopropylthiazole-4-carbonyl)-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)ethyl)phenethoxy)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / 2-methyltetrahydrofuran / 19.5 h / 31 - 50 °C

2: hydrogen bromide / toluene; water / 38 h / 87 °C / Reflux

3: potassium carbonate / acetonitrile; water / 66 h / 20 - 60 °C

4: N-benzyl-trimethylammonium hydroxide / acetonitrile; water / 1 h / 20 °C

With lithium aluminium tetrahydride; hydrogen bromide; N-benzyl-trimethylammonium hydroxide; potassium carbonate; In 2-methyltetrahydrofuran; water; toluene; acetonitrile;