5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

Base Information

Chemical Name:5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime
CAS No.:1429060-44-5
Molecular Formula:C₃₀H₃₂N₂O₅
Molecular Weight:500.594
Hs Code.:

Synonyms:5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

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Chemical Property of 5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

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Technology Process of 5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

There total 8 articles about 5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259391-09-7
5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxopropyl)-2-propoxy-benzaldehyde

: 1429060-44-5
5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; at 20 ℃;
DOI:10.1016/j.bmc.2013.02.003

Reference yield:

: 176047-66-8
benzyl 2-hydroxy-5-formylbenzoate

: 1429060-44-5
5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: sodium tetrahydroborate / ethanol / 2 h / 20 °C

3: phosphorus tribromide / diethyl ether / 1.5 h / 0 °C

4: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -50 - 0 °C

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

6: borane-THF / tetrahydrofuran / 0 °C

7: manganese(IV) oxide / dichloromethane / 20 °C

8: hydroxylamine hydrochloride; pyridine / ethanol / 20 °C

With pyridine; manganese(IV) oxide; sodium tetrahydroborate; borane-THF; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; phosphorus tribromide; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.02.003

Reference yield:

: 616-76-2
2-hydroxy-5-formylbenzoic acid

: 1429060-44-5
5-((R)-2-benzyl-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)-2-propoxybenzaldehyde oxime

Guidance literature:: Multi-step reaction with 9 steps

1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 60 °C

3: sodium tetrahydroborate / ethanol / 2 h / 20 °C

4: phosphorus tribromide / diethyl ether / 1.5 h / 0 °C

5: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -50 - 0 °C

6: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

7: borane-THF / tetrahydrofuran / 0 °C

8: manganese(IV) oxide / dichloromethane / 20 °C

9: hydroxylamine hydrochloride; pyridine / ethanol / 20 °C

With pyridine; manganese(IV) oxide; sodium tetrahydroborate; borane-THF; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; phosphorus tribromide; potassium carbonate; potassium hydrogencarbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.02.003