N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Base Information

• Chemical Name: N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine
• CAS No.: 1206195-86-9
• Molecular Formula: C₄₂H₅₀N₂O₅Si
• Molecular Weight: 690.955

Synonyms:N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Chemical Property of N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Chemical Property:

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Technology Process of N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

There total 7 articles about N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.6%

4-bromo-N,N-bis-(4-methoxyphenyl)aniline (194416-45-0) + N-[4-(3-{tert-butyl(dimethyl)silyloxy}propoxy)phenyl]-4-methoxyaniline (464216-82-8) → N1-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N1,N4,N4-tris(4-methoxyphenyl)benzene-1,4-diamine (1206195-86-9)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In toluene; at 90 ℃; Inert atmosphere;

Reference yield:

N,N-bis(4-methoxyphenyl)aniline (20440-94-2) → N1-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N1,N4,N4-tris(4-methoxyphenyl)benzene-1,4-diamine (1206195-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

2: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; tri-tert-butyl phosphine; sodium t-butanolate; In N,N-dimethyl-formamide; toluene;

Reference yield:

3-(4-Bromophenoxy)-1-propanol (67900-64-5) → N1-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N1,N4,N4-tris(4-methoxyphenyl)benzene-1,4-diamine (1206195-86-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 0.17 h / Inert atmosphere

2.2: 90 °C

3.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

With 1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In N,N-dimethyl-formamide; toluene;

upstream raw materials:

4-bromo-N,N-bis-(4-methoxyphenyl)aniline

N-[4-(3-{tert-butyl(dimethyl)silyloxy}propoxy)phenyl]-4-methoxyaniline

N,N-bis(4-methoxyphenyl)aniline

aniline

Downstream raw materials:

3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propan-1-ol

3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

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