3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

Base Information

Chemical Name:3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate
CAS No.:1206195-88-1
Molecular Formula:C₃₇H₃₈N₂O₇S
Molecular Weight:654.784
Hs Code.:

Synonyms:3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

Chemical Property:

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Technology Process of 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

There total 10 articles about 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.3%

: 1206195-87-0
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propan-1-ol

: 124-63-0
methanesulfonyl chloride

: 1206195-88-1
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

Guidance literature:: With dmap; triethylamine; Inert atmosphere; Cooling with ice;

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1206195-88-1
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: dmap / tetrahydrofuran / 0.17 h / Cooling with ice; Inert atmosphere

3.2: 0.17 h

3.3: 0.08 h

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; sodium t-butanolate; In tetrahydrofuran; toluene;

Reference yield:

: 1206195-86-9
N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

: 1206195-88-1
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / water; tetrahydrofuran

2: dmap; triethylamine / water; tetrahydrofuran

With dmap; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; water;