tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Base Information

Chemical Name:tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate
CAS No.:1380500-93-5
Molecular Formula:C₁₄H₁₇N₅O₂
Molecular Weight:287.321
Hs Code.:

Synonyms:tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Suppliers and Price of tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Chemical Property:

Purity/Quality:: >99.00% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

There total 13 articles about tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 66389-80-8
tert-butyl N-[(4-cyanophenyl)methyl]carbamate

: 3473-63-0
formamidine acetic acid

: 1380500-93-5
tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Guidance literature:: tert-butyl N-[(4-cyanophenyl)methyl]carbamate; formamidine acetic acid; With zinc trifluoromethanesulfonate; hydrazine; In N,N-dimethyl-formamide; at 30 ℃; for 36h; Microwave irradiation;

With hydrogenchloride; sodium nitrite; In water; N,N-dimethyl-formamide; at 20 ℃; pH=3;
DOI:10.1002/anie.201201117

Reference yield: 60.4%

: tert-butyl N-[[4-(1,2-dihydro-1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

: 1380500-93-5
tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Guidance literature:: With sodium nitrite; In dichloromethane; acetic acid; at 25 ℃; for 0.5h;
DOI:10.1021/jacs.0c11958

Reference yield: 40.0%

: 75-09-2
dichloromethane

: 66389-80-8
tert-butyl N-[(4-cyanophenyl)methyl]carbamate

: 1380500-93-5
tert-butyl N-[[4-(1,2,4,5-tetrazin-3-yl)phenyl]methyl]carbamate

Guidance literature:: dichloromethane; tert-butyl N-[(4-cyanophenyl)methyl]carbamate; With sulfur; hydrazine hydrate; In ethanol; at 50 ℃; for 24h; Microwave irradiation; Sealed tube;

With acetic acid; sodium nitrite; In ethanol; water; Sealed tube;
DOI:10.1002/anie.201804878