(Dimethylphenylsilyl)acetic acid ethyl ester

Base Information

Chemical Name:(Dimethylphenylsilyl)acetic acid ethyl ester
CAS No.:13950-56-6
Molecular Formula:C12H18 O2 Si
Molecular Weight:222.359
Hs Code.:
NSC Number:108054
DSSTox Substance ID:DTXSID20930491
Nikkaji Number:J303.523I
Wikidata:Q82905869
Mol file:13950-56-6.mol

Synonyms:13950-56-6;NSC108054;DTXSID20930491;Ethyl [dimethyl(phenyl)silyl]acetate;NSC-108054

Suppliers and Price of (Dimethylphenylsilyl)acetic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (Dimethylphenylsilyl)acetic acid ethyl ester

Chemical Property:

Vapor Pressure:0.00351mmHg at 25°C
Boiling Point:281.7°Cat760mmHg
Flash Point:105.7°C
Density:0.97g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:222.107606347
Heavy Atom Count:15
Complexity:208

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C[Si](C)(C)C1=CC=CC=C1

Technology Process of (Dimethylphenylsilyl)acetic acid ethyl ester

There total 6 articles about (Dimethylphenylsilyl)acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 105-36-2
ethyl bromoacetate

: 768-33-2
phenyldimethylsilyl chloride

: 13950-56-6
ethyl [2-(dimethylphenyl)silyl]ethanoate

Guidance literature:: With iodine; zinc; In diethyl ether; benzene; for 2.5h; Heating; i137;
DOI:10.1039/b201520j

Reference yield: 95.0%

: 141-78-6
ethyl acetate

: 768-33-2
phenyldimethylsilyl chloride

: 13950-56-6
ethyl [2-(dimethylphenyl)silyl]ethanoate

Guidance literature:: ethyl acetate; With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.75h; Inert atmosphere;

phenyldimethylsilyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4.5h; Inert atmosphere;
DOI:10.1246/cl.160975