1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

Base Information

Chemical Name:1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide
CAS No.:1373356-61-6
Molecular Formula:Br*C₂₀H₂₅N₂O₂
Molecular Weight:405.335
Hs Code.:

Synonyms:1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

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Chemical Property of 1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

Chemical Property:

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Technology Process of 1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

There total 3 articles about 1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 206446-42-6
tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate

: 1373356-61-6
1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

Guidance literature:: In acetonitrile; at 80 ℃; for 1h; Inert atmosphere;

Reference yield:

: 254454-54-1
tert-butyl-3-iodoazetidine-1-carboxylate

: 1373356-61-6
1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloro-trimethyl-silane; ethylene dibromide; zinc / N,N-dimethyl acetamide / 1.5 h / 20 - 65 °C / Inert atmosphere

1.2: 2 h / 80 °C / Inert atmosphere

2.1: acetonitrile / 1 h / 80 °C / Inert atmosphere

With chloro-trimethyl-silane; ethylene dibromide; zinc; In N,N-dimethyl acetamide; acetonitrile;

Reference yield:

: 15854-87-2
4-iodopyridine

: 1373356-61-6
1-benzyl-4-(1-(tert-butoxycarbonyl)azetidin-3-yl)pyridin-1-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloro-trimethyl-silane; ethylene dibromide; zinc / N,N-dimethyl acetamide / 1.5 h / 20 - 65 °C / Inert atmosphere

1.2: 2 h / 80 °C / Inert atmosphere

2.1: acetonitrile / 1 h / 80 °C / Inert atmosphere

With chloro-trimethyl-silane; ethylene dibromide; zinc; In N,N-dimethyl acetamide; acetonitrile;