(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Base Information

Chemical Name:(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide
CAS No.:865784-07-2
Molecular Formula:C₁₈H₂₁NO₇S
Molecular Weight:395.433
Hs Code.:

Synonyms:(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Suppliers and Price of (E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

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Technology Process of (E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

There total 7 articles about (E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 740835-10-3
2-(N-(3-hydroxy-4-methoxyphenyl)sulfamoyl)acetic acid

: 865784-07-2
(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Guidance literature:: With piperidine; benzoic acid; In toluene; for 4h; Reflux; Dean-Stark;
DOI:10.1021/jm400575x

Reference yield: 55.0%

: 908344-58-1
2-hydroxy-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethanesulfonamide

: 865784-07-2
(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 20 - 120 ℃; for 3h; Inert atmosphere; Dean-Stark;
DOI:10.1021/jm400575x

Reference yield:

: 1445727-01-4
ethyl 2-(N-(3-hydroxy-4-methoxyphenyl)sulfamoyl)acetate

: 865784-07-2
(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 3 h / 20 °C / Inert atmosphere

2: benzoic acid; piperidine / toluene / 4 h / Reflux; Dean-Stark

With piperidine; benzoic acid; sodium hydroxide; In water; toluene;
DOI:10.1021/jm400575x