(E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

Base Information

Chemical Name:(E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate
CAS No.:865784-24-3
Molecular Formula:C₁₈H₂₂NO₁₀PS
Molecular Weight:475.413
Hs Code.:

Synonyms:(E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

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Chemical Property of (E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

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Technology Process of (E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

There total 8 articles about (E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 865784-07-2
(E)-N-(3-hydroxy-4-methoxyphenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

: 865784-24-3
(E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

Guidance literature:: With triethylamine; trichlorophosphate; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jm400575x

Reference yield:

: 1687-53-2
5-amino-2-methoxyphenol

: 865784-24-3
(E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: sodium hydroxide / water / 3 h / 20 °C / Inert atmosphere

3: benzoic acid; piperidine / toluene / 4 h / Reflux; Dean-Stark

4: trichlorophosphate; triethylamine / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With piperidine; triethylamine; benzoic acid; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/jm400575x

Reference yield:

: 740835-10-3
2-(N-(3-hydroxy-4-methoxyphenyl)sulfamoyl)acetic acid

: 865784-24-3
(E)-2-methoxy-5-(2-(2,4,6-trimethoxyphenyl)vinylsulfonamido)phenyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: benzoic acid; piperidine / toluene / 4 h / Reflux; Dean-Stark

2: trichlorophosphate; triethylamine / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With piperidine; triethylamine; benzoic acid; trichlorophosphate; In tetrahydrofuran; toluene;
DOI:10.1021/jm400575x