[BiCl₃(1-(2-methoxybenzylidene)thiosemicarbazide)(H₂O)]*H₂O

Base Information

• Chemical Name: [BiCl₃(1-(2-methoxybenzylidene)thiosemicarbazide)(H₂O)]*H₂O
• CAS No.: 1335143-53-7
• Molecular Formula: C₉H₁₃BiCl₃N₃O₂S*H₂O
• Molecular Weight: 560.642
• Mol file: 1335143-53-7.mol

Synonyms:[BiCl₃(1-(2-methoxybenzylidene)thiosemicarbazide)(H₂O)]*H₂O

Chemical Property of [BiCl₃(1-(2-methoxybenzylidene)thiosemicarbazide)(H₂O)]*H₂O

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [BiCl₃(1-(2-methoxybenzylidene)thiosemicarbazide)(H₂O)]*H₂O

There total 1 articles about [BiCl₃(1-(2-methoxybenzylidene)thiosemicarbazide)(H₂O)]*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(naphthalen-2-ylmethylidene)hydrazinocarbothioamide (24091-06-3) + water (7732-18-5) + bismuth(III) chloride (7787-60-2) → [BiCl3(1-(2-methoxybenzylidene)thiosemicarbazide)(H2O)]*H2O (1335143-53-7)

Guidance literature:

In methanol; to a soln. of thiosemicarbazide-compound in hot methanol was added BiCl3, the soln. was heated under reflux for 2 h; filtered, washed with ethanol then ether and dried in vac. over CaCl2; elem. anal.;

DOI:10.1016/j.saa.2011.06.045

Reference yield:

[BiCl3(1-(2-methoxybenzylidene)thiosemicarbazide)(H2O)]*H2O (1335143-53-7) → bismuth (7440-69-9)

Guidance literature:

In neat (no solvent); byproducts: H2O, N2, C9H9N2OS; heating up to 1500°C under N2, heating rate of 10°C/min; TG;

DOI:10.1016/j.saa.2011.06.045

upstream raw materials:

2-(naphthalen-2-ylmethylidene)hydrazinocarbothioamide

water

bismuth(III) chloride

Downstream raw materials:

bismuth