C₂₆H₃₁ClN₄O₄

Base Information

Chemical Name:C₂₆H₃₁ClN₄O₄
CAS No.:1251527-67-9
Molecular Formula:C₂₆H₃₁ClN₄O₄
Molecular Weight:499.01
Hs Code.:

C<sub>26</sub>H<sub>31</sub>ClN<sub>4</sub>O<sub>4</sub>

Synonyms:C₂₆H₃₁ClN₄O₄

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Chemical Property of C₂₆H₃₁ClN₄O₄

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Technology Process of C₂₆H₃₁ClN₄O₄

There total 9 articles about C₂₆H₃₁ClN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13362-30-6
2-amino-4-ethoxycarbonyl-pyridine

: 1251529-11-9
1-[1-(4-chloro-3-methyl-benzyl)-piperidin-4-yl]-5-oxo-pyrrolidine-2-carboxylic acid

: 1251527-67-9
C₂₆H₃₁ClN₄O₄

Guidance literature:: 1-[1-(4-chloro-3-methyl-benzyl)-piperidin-4-yl]-5-oxo-pyrrolidine-2-carboxylic acid; With oxalyl dichloride; In dichloromethane; for 2h;

2-amino-4-ethoxycarbonyl-pyridine; pyridine; In dichloromethane; for 0.166667h;

Reference yield:

: 117890-58-1
4-(bromomethyl)-1-chloro-2-methylbenzene

: 1251527-67-9
C₂₆H₃₁ClN₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetonitrile / 14 h / 50 °C

2.1: molecular sieve 4A / N,N-dimethyl-formamide; acetic acid

3.1: trifluoroacetic acid / dichloromethane / 21 h / 25 °C

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.5 h

5.1: lithium hydroxide / 1,4-dioxane; water / 20 °C

6.1: oxalyl dichloride / dichloromethane / 2 h

6.2: 0.17 h

With oxalyl dichloride; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1251529-07-3
1-(4-chloro-3-methyl-benzyl)-piperidin-4-one

: 1251527-67-9
C₂₆H₃₁ClN₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: molecular sieve 4A / N,N-dimethyl-formamide; acetic acid

2.1: trifluoroacetic acid / dichloromethane / 21 h / 25 °C

3.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.5 h

4.1: lithium hydroxide / 1,4-dioxane; water / 20 °C

5.1: oxalyl dichloride / dichloromethane / 2 h

5.2: 0.17 h

With oxalyl dichloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;