N-benzyl-N-phenyl thioformamide

Base Information

Chemical Name:N-benzyl-N-phenyl thioformamide
CAS No.:36325-43-6
Molecular Formula:C₁₄H₁₃NS
Molecular Weight:227.33
Hs Code.:

Synonyms:N-benzyl-N-phenyl thioformamide

Suppliers and Price of N-benzyl-N-phenyl thioformamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-phenyl thioformamide

Chemical Property:

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Technology Process of N-benzyl-N-phenyl thioformamide

There total 4 articles about N-benzyl-N-phenyl thioformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 16350-99-5
N-benzylformanilide

: 36325-43-6
N-benzyl-N-phenyl thioformamide

Guidance literature:: With Lawessons reagent; In tert-butyl methyl ether; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/om500603v

Reference yield:

: 103-70-8
Formanilid

: 36325-43-6
N-benzyl-N-phenyl thioformamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / toluene / 2 h / 20 °C / Inert atmosphere

1.2: 3 h / 80 - 90 °C / Inert atmosphere

2.1: Lawessons reagent / tert-butyl methyl ether / 24 h / 20 °C / Inert atmosphere

With Lawessons reagent; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; In tert-butyl methyl ether; toluene;
DOI:10.1021/om500603v

Reference yield:

: 100-39-0
benzyl bromide

: 36325-43-6
N-benzyl-N-phenyl thioformamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / toluene / 2 h / 20 °C / Inert atmosphere

1.2: 3 h / 80 - 90 °C / Inert atmosphere

2.1: Lawessons reagent / tert-butyl methyl ether / 24 h / 20 °C / Inert atmosphere

With Lawessons reagent; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; In tert-butyl methyl ether; toluene;
DOI:10.1021/om500603v