4-(2-METHYL-4-THIAZOLYL)PHENOL*

Base Information

• Chemical Name: 4-(2-METHYL-4-THIAZOLYL)PHENOL*
• CAS No.: 30686-73-8
• Molecular Formula: C10H9 N O S
• Molecular Weight: 191.254
• Hs Code.: 2934100090
• Mol file: 30686-73-8.mol

Synonyms:Phenol,p-(2-methyl-4-thiazolyl)- (8CI); 4-(2-Methyl-1,3-thiazol-4-yl)phenol;4-(2-Methylthiazol-4-yl)phenol

Chemical Property of 4-(2-METHYL-4-THIAZOLYL)PHENOL*

Chemical Property:

• Vapor Pressure: 3.34E-05mmHg at 25°C
• Melting Point: 151℃ (ethanol )
• Refractive Index: 1.628
• Boiling Point: 344.3°C at 760 mmHg
• Flash Point: 162°C
• PSA: 61.36000
• Density: 1.257g/cm³
• LogP: 2.82410
• Sensitive.: Air Sensitive

Purity/Quality:

97% ^*data from raw suppliers

4-(2-Methyl-1,3-thiazol-4-yl)phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Potent peroxidase chemiluminescence enhancer for HRP.

Technology Process of 4-(2-METHYL-4-THIAZOLYL)PHENOL*

There total 8 articles about 4-(2-METHYL-4-THIAZOLYL)PHENOL* which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-bromo-1-(4'-hydroxyphenyl)-1-ethanone (2491-38-5) + thioacetamide (62-55-5) → 4-(4-hydroxyphenyl)-2-methylthiazole (30686-73-8)

Guidance literature:

In ethanol; for 4h; Reflux;

DOI:10.2174/1570178613666161017111615

Reference yield: 70.0%

methyl 4-(2-methyl-1,3-thiazol-4-yl)phenyl ether (50834-78-1) → 4-(4-hydroxyphenyl)-2-methylthiazole (30686-73-8)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1016/S0928-0987(02)00024-6

Reference yield:

acetic acid 4-(2-bromoacetyl)phenyl ester (41104-10-3) + thioacetamide (62-55-5) → 4-(4-hydroxyphenyl)-2-methylthiazole (30686-73-8)

Guidance literature:

With potassium hydroxide; In methanol; ethanol;

upstream raw materials:

methyl 4-(2-methyl-1,3-thiazol-4-yl)phenyl ether

2-Bromo-4'-methoxyacetophenone

acetic acid 4-(2-bromoacetyl)phenyl ester

thioacetamide

Downstream raw materials:

ethyl (R,S)-2-{[4-(2-methyl-1,3-thiazol-4-yl)phenyl]oxy}-5-phenylpent-4-enoate

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