Technology Process of methyl 2-benzoyl-4-fluorobenzoate
There total 4 articles about methyl 2-benzoyl-4-fluorobenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 4h;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diethyl ether; tetrahydrofuran / 0.75 h / -78 - 20 °C
1.2: 20 °C
2.1: Dess-Martin periodane / dichloromethane / 1 h
3.1: triethylamine / 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct / N,N-dimethyl-formamide / 4 h / 80 °C / 760.05 Torr
With
Dess-Martin periodane; triethylamine;
1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Dess-Martin periodane / dichloromethane / 1 h
2: triethylamine / 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct / N,N-dimethyl-formamide / 4 h / 80 °C / 760.05 Torr
With
Dess-Martin periodane; triethylamine;
1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct;
In
dichloromethane; N,N-dimethyl-formamide;
