chloro(trichloromethyl)diphenylgermane

Base Information

Chemical Name:chloro(trichloromethyl)diphenylgermane
CAS No.:1278557-77-9
Molecular Formula:C₁₃H₁₀Cl₄Ge
Molecular Weight:380.624
Hs Code.:

Synonyms:chloro(trichloromethyl)diphenylgermane

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Chemical Property of chloro(trichloromethyl)diphenylgermane

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Technology Process of chloro(trichloromethyl)diphenylgermane

There total 2 articles about chloro(trichloromethyl)diphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 56-23-5
tetrachloromethane

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

: 1278557-77-9
chloro(trichloromethyl)diphenylgermane

: 7366-23-6
diphenylchlorogermane

: 1613-66-7
dichlorodiphenylgermane

Guidance literature:: In tetrahydrofuran-d8; High Pressure; photolysis at 254 nm;
DOI:10.1139/V10-082

Reference yield: 11.0%

: 25105-16-2
trichloro(trichloromethyl)germane

: 100-58-3
phenylmagnesium bromide

: 1278557-77-9
chloro(trichloromethyl)diphenylgermane

Guidance literature:: In diethyl ether; (N2) to Cl3GeCCl3 in Et2O PhMgBr in ether was added dropwise, stirred atroom temp. for 2 h; solvent was removed in vacuo, residue was washed with pentane, washes were evapd. in vacuo and distilled at 110-120°C and 0.05 mm Hg;
DOI:10.1139/V10-082