2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

Base Information

Chemical Name:2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane
CAS No.:74075-29-9
Molecular Formula:C₂₃H₂₇NO₅
Molecular Weight:397.471
Hs Code.:

Synonyms:2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

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Chemical Property of 2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

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Technology Process of 2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

There total 4 articles about 2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.9%

: 98-88-4
benzoyl chloride

: 74075-28-8
(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

: 74075-29-9
2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

Guidance literature:: In pyridine; for 72h; Ambient temperature;
DOI:10.1021/jm00186a020

Reference yield:

: 33861-65-3
N-phthaloyl-L-phenylalanine-2-mercaptopyridyl thioester

: 74075-29-9
2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) magnesium / 1.) THF, from 30 deg C to 35 deg C, 1 h, 2.) THF, RT, 20 h

2: 58 percent / p-toluenesulfonyl chloride / toluene / 11 h

3: 1.3 g / hydrazine / ethanol / 0.25 h / Heating

4: 72.9 percent / pyridine / 72 h / Ambient temperature

With magnesium; p-toluenesulfonyl chloride; hydrazine; In pyridine; ethanol; toluene;
DOI:10.1021/jm00186a020

Reference yield:

: 74075-26-6
2-(3-oxo-5-phenyl-(4S)-4-phthalimidopentyl)-1,3-dioxolane

: 74075-29-9
2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-benzamido-2-phenylethyl>-1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / p-toluenesulfonyl chloride / toluene / 11 h

2: 1.3 g / hydrazine / ethanol / 0.25 h / Heating

3: 72.9 percent / pyridine / 72 h / Ambient temperature

With p-toluenesulfonyl chloride; hydrazine; In pyridine; ethanol; toluene;
DOI:10.1021/jm00186a020