Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester

Base Information

• Chemical Name: Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester
• CAS No.: 102839-81-6
• Molecular Formula: C₂₄H₂₃NO₃
• Molecular Weight: 373.452
• Mol file: 102839-81-6.mol

Synonyms:Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester

Chemical Property of Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester

There total 3 articles about Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

diphenyl(2-phenyl-aziridin-2-yl)methanol (64889-89-0) + chloroformic acid ethyl ester (541-41-3) → Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester (102839-81-6)

Guidance literature:

With triethylamine; In diethyl ether; at -5 ℃; for 12h;

DOI:10.1016/S0040-4039(00)88298-2

Reference yield:

1-hydroxy-1,1-diphenylpropan-2-one oxime (7474-15-9) → Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester (102839-81-6)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: 96 percent / Et₃N / diethyl ether / 12 h / -5 °C

With triethylamine; In diethyl ether; toluene;

DOI:10.1016/S0040-4039(00)88298-2

Reference yield:

1-phenyl-1,2-propanedione 2-oxime (119-51-7) → Carbonic acid diphenyl-(2-phenyl-aziridin-2-yl)-methyl ester ethyl ester (102839-81-6)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: toluene

3: 96 percent / Et₃N / diethyl ether / 12 h / -5 °C

With triethylamine; In diethyl ether; toluene;

DOI:10.1016/S0040-4039(00)88298-2

upstream raw materials:

diphenyl(2-phenyl-aziridin-2-yl)methanol

chloroformic acid ethyl ester

1-hydroxy-1,1-diphenylpropan-2-one oxime

1-phenyl-1,2-propanedione 2-oxime

Downstream raw materials:

2,2,3-triphenyl-1-azabicyclo<1.1.0>butane

2,3,3-triphenylacrylaldehyde

4,4,5-Triphenyl-3-oxa-1-aza-bicyclo[3.1.0]hexan-2-one