1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

Base Information

Chemical Name:1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine
CAS No.:754978-61-5
Molecular Formula:C₃₄H₃₄N₂O₉
Molecular Weight:614.652
Hs Code.:

Synonyms:1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

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Technology Process of 1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

There total 2 articles about 1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 754978-60-4
3,5-di-O-benzyl-1,2-di-O-isopropylidene-3-C-hydroxymethyl-α-D-ribofuranose

: 108-24-7
acetic anhydride

: 98-88-4
benzoyl chloride

: 65-71-4,28806-14-6,691841-57-3
thymin

: 754978-61-5
1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

Guidance literature:: Multistep reaction;
DOI:10.1021/jo0491861

Reference yield:

: 207606-87-9
1,2-di-O-isopropylidene-3,5-di-O-benzyl-3-C-vinyl-α-D-ribofuranose

: 754978-61-5
1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

Guidance literature:: DOI:10.1021/jo0491861

Reference yield: 100.0%

: 754978-61-5
1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine

: 124-63-0
methanesulfonyl chloride

: 754978-62-6
1-(3,5-di-O-benzyl-2-O-methanesulfonyl-3-C-(methanesulfonyl-oxy)methyl-β-D-ribofuranosyl)thymine

Guidance literature:: 1-(2-O-acetyl-3-C-(benzoyloxy)methyl-3,5-di-O-benzyl-β-D-ribofuranosyl)thymine; With sodium methylate; In methanol; at 20 ℃;

methanesulfonyl chloride; With pyridine; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo0491861