5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo

Base Information

Chemical Name:5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo
CAS No.:115775-87-6
Molecular Formula:C₅₆H₅₂MnN₄O
Molecular Weight:851.993
Hs Code.:

Synonyms:5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo

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Chemical Property of 5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo

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Technology Process of 5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo

There total 7 articles about 5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: tetramethyl ammonium hydroxide

: 85939-49-7
(5,10,15,20-tetramesitylporphyrinato)manganese(III) chloride

: 937-14-4
3-chloro-benzenecarboperoxoic acid

: 115775-87-6
5,10,15,20-tetramesitylporphyrin?manganese(IV)-oxo

Guidance literature:: In methanol; dichloromethane; after cooling to 0°C addn. of m-CPBA, stirring for 1min at 0°C; chromy. at -78°C on a basic alumina column (CH2Cl2/ethyl acetate 1:1), evapn. of the solvent at -78°C and drying of the precipitate in vac. at room temp.;
DOI:10.1021/ja00234a009