Technology Process of 2-(3,5-dimethoxyphenyl)-6-methoxybenzofuran
There total 4 articles about 2-(3,5-dimethoxyphenyl)-6-methoxybenzofuran which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodine; potassium carbonate;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/anie.202006542
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
Heating;
DOI:10.1248/cpb.39.579
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium nitrite; hydrogenchloride / ethanol; water / 2.17 h / 0 °C / Schlenk technique; Inert atmosphere
2: potassium carbonate / acetone; dichloromethane / 7 h / 55 °C / Schlenk technique; Inert atmosphere; Sealed tube
3: potassium carbonate; iodine / tetrahydrofuran / 2 h / 20 °C / Schlenk technique; Inert atmosphere
With
hydrogenchloride; iodine; potassium carbonate; sodium nitrite;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone;
DOI:10.1002/anie.202006542
