2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

Base Information

Chemical Name:2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane
CAS No.:808739-73-3
Molecular Formula:C₂₇H₄₀O₅SSi
Molecular Weight:504.763
Hs Code.:

Synonyms:2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

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Chemical Property of 2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

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Technology Process of 2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

There total 3 articles about 2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 107-21-1
ethylene glycol

: 808739-72-2
6-[4-(tert-butyldimethylsilyloxy)phenyl]-4-[(4-methylphenyl)sulfonyl]hexan-2-one

: 808739-73-3
2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 2.5h; Heating;
DOI:10.1055/s-2004-831240

Reference yield:

: 147974-20-7
3-[4-(tert-butyl-dimethyl-silanyloxy)phenyl]propionaldehyde

: 808739-73-3
2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / K₂CO₃; 18-crown-6 / toluene / 2 h / Heating

2: 90 percent / AcOH / ethanol / 48 h / 20 °C

3: 80 percent / p-TsOH / toluene / 2.5 h / Heating

With 18-crown-6 ether; potassium carbonate; toluene-4-sulfonic acid; acetic acid; In ethanol; toluene; 1: Wittig reaction;
DOI:10.1055/s-2004-831240

Reference yield:

: 808739-71-1
(3E)-6-[4-(tert-butyldimethylsilyloxy)phenyl]hex-3-en-2-one

: 808739-73-3
2-({4-[4-(tert-butyldimethylsilyloxy)phenyl]}-2-[(4-methylphenyl)sulfonyl]butyl)-2-methyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / AcOH / ethanol / 48 h / 20 °C

2: 80 percent / p-TsOH / toluene / 2.5 h / Heating

With toluene-4-sulfonic acid; acetic acid; In ethanol; toluene;
DOI:10.1055/s-2004-831240